OLEFIN DIHYDROXYLATION MEDIATED BY OS-ZN-AL HYDROTALCITE-LIKE CATALYST: THE SCOPE AND REACTIVITY USING VARIOUS CO-OXIDANTS

Olefin dihydroxylation mediated by Os-Zn-Al hydrotalcite-like catalyst: The scope and reactivity using various co-oxidants

The heterogeneous oxidation of olefins to vicinal diols was investigated using an Os-Zn-Al hydrotalcite-like catalyst (HTlc).The Os-Zn-Al HTlc was synthesised by the co-precipitation method and characterised fully using XRD, FT-IR, TEM, SEM, ICP-OES and BET surface area measurements.The ability of the synthesised Os-Zn-Al HTlc to catalytically dihy

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Measuring deuterium permeation through tungsten near room temperature under plasma loading using a getter layer and ion-beam based detection

A method to measure deuterium permeation through tungsten near room temperature under plasma loading is presented.The permeating deuterium is accumulated in a getter layer of zirconium, titanium or erbium, respectively, on the unexposed side of the sample.Subsequently, the amount of deuterium in the getter is measured ex-situ using Face Mask nuclea

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